15.9.2009 |
EN |
Official Journal of the European Union |
L 242/14 |
COMMISSION DIRECTIVE 2009/122/EC
of 14 September 2009
amending, for the purposes of its adaptation to technical progress, Annex II to Directive 96/73/EC of the European Parliament and of the Council on certain methods for quantitative analysis of binary textile fibre mixtures
(Text with EEA relevance)
THE COMMISSION OF THE EUROPEAN COMMUNITIES,
Having regard to the Treaty establishing the European Community,
Having regard to Directive 96/73/EC of the European Parliament and of the Council of 16 December 1996 on certain methods for quantitative analysis of binary textile fibre mixtures (1), and in particular Article 5 thereof,
Whereas:
(1) |
Directive 2008/121/EC of the European Parliament and the Council of 14 January 2009 on textile names (2) requires labelling to indicate the fibre composition of textile products, with checks being carried out by analysis on the conformity of these products with indications given on the label. |
(2) |
Uniform methods for quantitative analysis of binary textile fibre mixtures are provided for in Directive 96/73/EC. |
(3) |
On the basis of recent findings by the technical working group, Directive 2008/121/EC was adapted to technical progress, by adding the fibre melamine to the list of fibres set out in Annexes I and V to that Directive. |
(4) |
It is therefore, necessary to define uniform test methods for melamine. |
(5) |
Directive 96/73/EC should therefore be amended accordingly. |
(6) |
The measures provided for in this Directive are in accordance with the opinion of the Committee for Directives relating to Textile Names and Labelling, |
HAS ADOPTED THIS DIRECTIVE:
Article 1
Annex II to Directive 96/73/EC is amended in accordance with the Annex to this Directive.
Article 2
Transposition
1. Member States shall bring into force the laws, regulations and administrative provisions necessary to comply with this Directive by 15 September 2010 at the latest. They shall forthwith communicate to the Commission the text of those provisions and a correlation table between those provisions and this Directive.
When Member States adopt those provisions, they shall contain a reference to this Directive or be accompanied by such a reference on the occasion of their official publication. Member States shall determine how such reference is to be made.
2. Member States shall communicate to the Commission the text of the main provisions of national law which they adopt in the field covered by this Directive.
Article 3
This Directive shall enter into force on the 20th day following its publication in the Official Journal of the European Union.
Article 4
This Directive is addressed to the Member States.
Done at Brussels, 14 September 2009.
For the Commission
Günter VERHEUGEN
Vice-President
ANNEX
Chapter 2 of Annex II to Directive 96/73/EC is amended as follows:
(a) |
the Special Methods — Summary Table is replaced by the following: ‘SUMMARY TABLE
|
(b) |
method No 1 is amended as follows:
|
(c) |
method No 2 is amended as follows:
|
(d) |
method No 3 is amended as follows:
|
(e) |
method No 4 is amended as follows:
|
(f) |
method No 5 is amended as follows:
|
(g) |
method No 6 is amended as follows:
|
(h) |
method No 8 is amended as follows:
|
(i) |
method No 9 is amended as follows:
|
(j) |
point 1.2 of method No 10 is replaced by the following:
|
(k) |
method No 11 is amended as follows:
|
(l) |
method No 13 is amended as follows:
|
(m) |
method No 14 is amended as follows:
|
(n) |
method No 15 is amended as follows:
|
(o) |
method No 16 is inserted after method No 15: ‘ METHOD No 16 MELAMINE AND CERTAIN OTHER FIBRES (Method using hot formic acid) 1. FIELD OF APPLICATION This method is applicable, after removal of non-fibrous matter, to binary mixtures of:
2. PRINCIPLE The melamine is dissolved out from a known dry mass of the mixture with hot formic acid (90 % by mass). The residue is collected, washed, dried and weighed; its mass, corrected if necessary, is expressed as a percentage of the dry mass of the mixture. The percentage of the second constituents is obtained by difference. Note: Keep strictly the recommended temperature range because the solubility of melamine is very much dependent on temperature. 3. APPARATUS AND REAGENTS (other than those specified in the general instructions) 3.1. Apparatus
3.2. Reagents
4. TEST PROCEDURE Follow the procedure described in the general instructions, then proceed as follows: To the specimen contained in the glass-stoppered conical flask of at least 200 ml capacity, add 100 ml of formic acid per gram of specimen. Insert the stopper and shake the flask to wet out the specimen. Maintain the flask in a shaking water bath at 90 ± 2 °C for 1 hour, shaking it vigorously. Cool the flask to room temperature. Decant the liquid through the weighed filter crucible. Add 50 ml of formic acid to the flask containing the residue, shake manually and filter the contents of the flask through the filter crucible. Transfer any residual fibres to the crucible by washing out the flask with a little more formic acid reagent. Drain the crucible with suction and wash the residue with formic acid reagent, hot water, dilute ammonia solution, and finally cold water, draining the crucible with suction after each addition. Do not apply suction until each washing liquor has drained under gravity. Finally, drain the crucible with suction, dry the crucible and residue, and cool and weigh them. Note: Temperature has a very strong influence on solubility properties of melamine and should be carefully controlled. 5. CALCULATION AND EXPRESSION OF RESULTS Calculate the results as described in the general instructions. The value of “d” for cotton and aramid is 1,02. 6. PRECISION On a homogeneous mixture of textile materials, the confidence limits of results obtained by this method are not greater than ± 2 for a confidence level of 95 %.’ |
Ключевые слова
- маркировка
- аналитическая химия
- текстильное волокно
- текстильное изделие
- пластмассы
- искусственное волокно
- натуральное волокно
- количественный анализ
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